A Thin Film Preparation Using Focused High Power Ion

نویسندگان

  • M. Bystritskii
  • S. N. Volkov
  • A. V. Mytnikov
  • A. A. Sinebryukhov
  • D. J. Rej
چکیده

Among the well known physical methods of thin film preparation as target evaporation by magnetron irradiation, by laser, electron and long pulse ion beams, the method of precipitation of evaporated target material with short pulse ( < 100 ns) and high power (>10 W/cm) ion beam seems to be less investigated. The advantages of such method are: 1. high precipitation velocity ( 1 Jlm per shot); 2. possibility offilm formation at high area substrate ( 100 cm); 3. moderate vacuum conditions needed (10" 10" Torr) two order higher compared to other methods; 4. high melting temperature target usage. These advantages are provided by action of pulsed ion beam at the target, when the effective energy transfer into target occurs, but irradiation energy losses are minimal. The thickness of evaporated layer of the target is determined by ion range in material (usually 1 10 Jlm) providing high velocity precipitation. Pulsed action of target plasma results in thermal and mechanical dynamic loading, that is important for film properties. The usage of described method for formation of diamond like is of the most interest. In order to precipitate the carbon films we used high power ion beam with the following parameters: E = 600 keV, I= 60 kA, t =80 ns. Ion beam was generated in focusing B-applied diode at GIMN accelerator. The ion beam consisted of approximately 70% of protons and 30% of carbon ions. The ion current density in the focal plane reached 9 kA/cm that corresponds to 300 J/cm. Thickness of the precipitated films made up to 100 nm per shot at the distance between target and substrate 4 em. In the case of glass substrate, its surface layer was strongly destructed. The electrical resistance of film was at the level of 100 Ohm. In the report the ellypsometric data obtained with scanning electron microscope are given.

برای دانلود رایگان متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Preparation of plan-view Co-doped FeSi thin film TEM specimens using FIB

When examining thin films using transmission electron microscopy (TEM), it is usually necessary to image a cross-section of the film (i.e. parallel to the film). However sometimes it is favourable to image thin films in plan-view (i.e. perpendicular to the film). This is the case for Co-doped FeSi thin films, which possess chiral symmetry along certain zone axes. In order to view these zone axe...

متن کامل

FIB Sample Preparation of Polymer Thin Films on Hard Substrates Using the Shadow-FIB Method

Focused ion beam (FIB) instrumentation has proven to be extremely useful for preparing cross-sectional samples for transmission electron microscopy (TEM) investigations. The two most widely used methods involve milling a trench on either side of an electron-transparent window: the “H-bar” and the “lift-out” methods [1]. Although these two methods are very powerful in their versatility and abili...

متن کامل

Preparation of high-quality planar FeRh thin films for in situ TEM investigations

The preparation of a planar FeRh thin film using a focused ion beam (FIB) secondary electron microscope (SEM) for the purpose of in situ transmission electron microscopy (TEM) is presented. A custom SEM stub with 45° faces allows for the transfer and milling of the sample on a TEM heating chip, whilst Fresnel imaging within the TEM revealed the presence of the magnetic domain walls, confirming ...

متن کامل

Preparation and proposed mechanism of ZnO Nanostructure Thin Film on Glass with Highest c-axis Orientation

In this paper, ZnO thin film is deposited on slide glass substrate using the sol-gel process. Presenting well-defined orientation of ZnO thin films Nanostructure were obtained by dip coating of zinc acetate dihydrate, monoethanolamine (MEA), de-ionized water and isopropanol alcohol. The annealed ZnO thin films were transparent ca 85-90% in visible range with an absorption edges at about 375 nm....

متن کامل

SnO2 Nanowires on Carbon Nanotube Film as a High Performance Anode Material for Flexible Li-ion Batteries

Today, Li-ion batteries (LIBs) are the most common rechargeable batteries used in electronic devices. SnO2 with theoretical specific capacity of 782 mAh/g is among the best anode materials for LIBs. In this report, Three-dimensional SnO2 nanowires (NWs) on carbon nanotube (CNT) thin film (SnO2 / CNT) is fabricated using a combination of vacuum filtration and thermal evaporation techniques. The ...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2015